Quantitative 13C NMR Characterization of Fast Pyrolysis Oils

Jack Ferrell; Renee Happs; Maarit Iisa

doi:10.1039/C6RA24044E

Quantitative 13C NMR Characterization of Fast Pyrolysis Oils

Jack Ferrell, Renee Happs, Maarit Iisa

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21 Scopus Citations

Abstract

Quantitative ¹³C NMR analysis of model catalytic fast pyrolysis (CFP) oils following literature procedures showed poor agreement for aromatic hydrocarbons between NMR measured concentrations and actual composition. Modifying integration regions based on DEPT analysis for aromatic carbons resulted in better agreement. Solvent effects were also investigated for hydrotreated CFP oil.

Original language	American English
Pages (from-to)	102665-102670
Number of pages	6
Journal	RSC Advances
Volume	6
Issue number	104
DOIs	https://doi.org/10.1039/C6RA24044E https://doi.org/10.1039/c6ra24044e
State	Published - 2016

Bibliographical note

Publisher Copyright:
© 2016 The Royal Society of Chemistry.

NREL Publication Number

NREL/JA-5100-67305

Keywords

13C
catalytic fast pyrolysis
NMR
pyrolysis

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title = "Quantitative 13C NMR Characterization of Fast Pyrolysis Oils",

abstract = "Quantitative 13C NMR analysis of model catalytic fast pyrolysis (CFP) oils following literature procedures showed poor agreement for aromatic hydrocarbons between NMR measured concentrations and actual composition. Modifying integration regions based on DEPT analysis for aromatic carbons resulted in better agreement. Solvent effects were also investigated for hydrotreated CFP oil.",

keywords = "13C, catalytic fast pyrolysis, NMR, pyrolysis",

author = "Jack Ferrell and Renee Happs and Maarit Iisa",

note = "Publisher Copyright: {\textcopyright} 2016 The Royal Society of Chemistry.",

year = "2016",

doi = "10.1039/C6RA24044E",

language = "American English",

volume = "6",

pages = "102665--102670",

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T1 - Quantitative 13C NMR Characterization of Fast Pyrolysis Oils

AU - Ferrell, Jack

AU - Happs, Renee

AU - Iisa, Maarit

PY - 2016

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N2 - Quantitative 13C NMR analysis of model catalytic fast pyrolysis (CFP) oils following literature procedures showed poor agreement for aromatic hydrocarbons between NMR measured concentrations and actual composition. Modifying integration regions based on DEPT analysis for aromatic carbons resulted in better agreement. Solvent effects were also investigated for hydrotreated CFP oil.

AB - Quantitative 13C NMR analysis of model catalytic fast pyrolysis (CFP) oils following literature procedures showed poor agreement for aromatic hydrocarbons between NMR measured concentrations and actual composition. Modifying integration regions based on DEPT analysis for aromatic carbons resulted in better agreement. Solvent effects were also investigated for hydrotreated CFP oil.

KW - 13C

KW - catalytic fast pyrolysis

KW - NMR

KW - pyrolysis

UR - http://www.scopus.com/inward/record.url?scp=84994031574&partnerID=8YFLogxK

U2 - 10.1039/C6RA24044E

DO - 10.1039/C6RA24044E

M3 - Article

AN - SCOPUS:84994031574

SN - 2046-2069

VL - 6

SP - 102665

EP - 102670

JO - RSC Advances

JF - RSC Advances

IS - 104

ER -

Quantitative 13C NMR Characterization of Fast Pyrolysis Oils

Abstract

Bibliographical note

NREL Publication Number

Keywords

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